3-Cyanophenol → HCID 81828420, compound

HRID 873059Notes

Reaction equation

HRID 873059 reaction equation
F[C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=1[C:10]([F:13])([F:12])[F:11].[OH:14][C:15]1[CH:16]=[C:17]([CH:20]=[CH:21][CH:22]=1)[C:18]#[N:19]>>[CH:6]([C:5]1[CH:8]=[CH:9][C:2]([O:14][C:15]2[CH:16]=[C:17]([CH:20]=[CH:21][CH:22]=2)[C:18]#[N:19])=[C:3]([C:10]([F:13])([F:12])[F:11])[CH:4]=1)=[O:7]

Participants

3

Reactant 2

HCID 133943-CyanophenolHCID 5222694-Fluoro-3-(trifluoromethyl)benzaldehyde

Product 1

HCID 81828420HCID 81828420, compound

Procedure

The title compound was prepared by a procedure similar to that described for D4 starting from 4-fluoro-3-(trifluoromethyl)benzaldehyde and 3-hydroxybenzonitrile. LC-MS (ESI): m/z 290 [M−H]−; 1.69 min (ret time).

Workup

  1. custom1.69 min (ret time)

Sources & evidence

ORD record
ord-d31027f0029e420a85137b1a6d848e0b
Source dataset
uspto-grants-2015_03
Patent number
US08975400B2

Reaction notes

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