HCID 86724193, compound → HCID 86724195, compound

Participants

Reaction Steps

To a solution of 2-((2-chloropyridin-4-yl)oxy)-5-formylbenzonitrile (400 mg, 1.55 mmol) and dicyanozinc (182 mg, 1.55 mmol) in N,N-dimethylacetamide (DMA) (4 mL) was added tetrakis(triphenylphosphine)palladium(0) (179 mg, 0.155 mmol). The reaction mixture was sealed in a microwave vial and irradiated with a microwave using initial normal to 100° C. for 1 h and filtered.

Provenance & Evidence