HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71241201, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 71239623 | HCID 71239623 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 71241201 | HCID 71241201 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using sodium hydride (12.28 mg, 0.307 mmol), 5-(hydroxymethyl)-2-((2-(trifluoromethyl)pyridin-4-yl)oxy)benzonitrile (60.2 mg, 0.205 mmol) in THF (8 mL) and 7-chloro-1-methyl-2,3-dihydroimidazo-[1,2-c]pyrimidin-5(1H)-one (38 mg, 0.205 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-322c078a08fa4500952acb63fe452231 |
| Source note | uspto-grants-2015_03 |