HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 86724209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Reactant | HCID 86724191 | HCID 86724191 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86724209 | HCID 86724209 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using 7-chloro-1-methyl-2,3-dihydroimidazo[1,2-c]pyrimidin-5(1H)-one (60 mg, 0.323 mmol), sodium hydride (25.9 mg, 0.647 mmol) and 2-((6-chloropyridin-3-yl)oxy)-5-(hydroxymethyl)benzonitrile (84 mg, 0.323 mmol) in DMF (2 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-fb00698f5f5749fdad94a4545d70695e |
| Source note | uspto-grants-2015_03 |