HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71243775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-(4-(5-(Trifluoromethyl)-2-pyridinyloxy)phenyl)ethanol | HCID 19017550 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 71243775 | HCID 71243775 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using 7-chloro-1-methyl-2,3-dihydroimidazo[1,2-c]pyrimidin-5(1H)-one (50 mg, 0.269 mmol), sodium hydride (21.55 mg, 0.539 mmol) and 2-(4-((5-(trifluoromethyl)pyridin-2-yl)oxy)phenyl)ethanol (76 mg, 0.269 mmol) in DMF (1 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-be96652fc6ea494dbb47aa59f29b6d43 |
| Source note | uspto-grants-2015_03 |