HCID 117702730, compound → HCID 86294278, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-((4-chlorophenyl)(3-methylbenzo[d]isoxazol-5-ylamino)methyl)-1,5-dimethyl-1H-pyrazole-3-carboxylic acid (Step 33.5). tR: 4.70 min (HPLC 1); tR: 1.03 min (LC-MS 2); ESI-MS: 393 [M+H]+ (LC-MS 2); Rf=0.50 (CH2Cl2/MeOH 9:1); 1H NMR (400 MHz, DMSO-d6) δ ppm 2.08 (s, 3H) 2.44-2.57 (m, 3H) 3.85 (s, 3H) 6.52 (s, 1H) 7.29 (s, 4H) 7.63 (d, J=9.0 Hz, 1H) 7.73 (dd, J=9.0, 2.0 Hz, 1H) 8.01 (d, J=1.6 Hz, 1H).

Provenance & Evidence