HCID 117702866, compound → HCID 86294479, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-((4-chlorophenyl)((1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)amino)methyl)-1-cyclopropyl-1H-pyrazole-3-carboxylic acid (Step 39.2). tR: 3.88 min (HPLC 1); tR: 0.88 min (LC-MS 2); ESI-MS: 395 [M+H]+ (LC-MS 2); Rf=0.33 (CH2Cl2/MeOH 9:1); 1H NMR (400 MHz, DMSO-d6) δ ppm 0.96-1.04 (m, 2H) 1.08-1.14 (m, 2H) 1.90 (s, 3H) 3.34 (s, 3H) 3.83-3.91 (m, 1H) 6.11 (s, 1H) 7.18-7.23 (m, 2H) 7.30-7.38 (m, 3H) 7.68-7.71 (m, 1H) 7.88 (s, 1H).

Provenance & Evidence