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HRID873873

反应详情

EQUATION

反应方程式

HRID 873873 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(N)cn(C)c1=O
HCID67456616

未命名化合物

结构：CCOC(=O)c1nn(C2CC2)c(C(F)(F)F)c1C(O)c1ccc(Cl)cc1
HCID117702816

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1nn(C2CC2)c(C(F)(F)F)c1C(Nc1cc(C)c(=O)n(C)c1)c1ccc(Cl)cc1
HCID117702946

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.ClCCl
溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 10.3 using ethyl 4-((4-chlorophenyl)(hydroxy)methyl)-1-cyclopropyl-5-(trifluoromethyl)-1H-pyrazole-3-carboxylate (Step 40.2) and 5-amino-1,3-dimethylpyridin-2(1H)-one (Step 20.2) at RT for 4 days. tR: 1.22 min (LC-MS 2); ESI-MS: 509 [M+H]+ (LC-MS 2); Rf=0.32 (5% MeOH/CH2Cl2).