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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 873896Generated: October 30, 2026

5-Amino-3-chloro-1-methyl-1,2-dihydropyridin-2-one → HCID 117702832, compound

https://huagongshe.com/reaction/873896

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Amino-3-chloro-1-methyl-1,2-dihydropyridin-2-oneHCID 71756073—
ReactantHCID 117702714HCID 117702714—
SolventEthyl AcetateHCID 8857—
ProductHCID 117702832HCID 117702832—

Reaction Steps

The title compound was prepared in analogy to the procedure described in Step 10.3 using ethyl 4-((4-chlorophenyl)(hydroxy)methyl)-1-(2,4-dimethoxypyrimidin-5-yl)-3-methyl-1H-pyrazole-5-carboxylate (Step 52.3) and 5-amino-3-chloro-1-methylpyridin-2(1H)-one (Step 5.2). tR: 4.89 min (HPLC 1); tR: 1.12 min (LC-MS 2); ESI-MS: 573/575 [M+H]+ (LC-MS 2); Rf=0.21 (EtOAc).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08975417B2
Source datasetuspto-grants-2015_03
ORD IDord-10c23b5a2a7841d2971363a83637baaa
Source noteuspto-grants-2015_03