HCID 117702674, compound → HCID 86291795, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-((4-chlorophenyl)((3-methylbenzo[d]isoxazol-5-yl)amino)methyl)-1-(2,4-dimethoxypyrimidin-5-yl)-5-isopropyl-1H-pyrazole-3-carboxylic acid (Step 54.2).; tR: 1.21 min (LC-MS 2); ESI-MS: 545 [M+H]+ (LC-MS 2); Rf=0.50 (EtOAc); 1H NMR (400 MHz, DMSO-d6) δ ppm 0.48 (d, J=6.8 Hz, 3H) 1.17 (d, J=7.0 Hz, 3H) 2.54 (s, 3H) 2.61-2.71 (m, 1H) 3.96 (s, 3H) 4.01 (s, 3H) 6.71 (s, 1H) 7.31-7.42 (m, 4H) 7.67 (d, J=8.9 Hz, 1H) 7.80 (dd, J=8.9, 2.0 Hz, 1H) 8.04 (d, J=1.8 Hz, 1H).

Provenance & Evidence