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HRID873950

反应详情

EQUATION

反应方程式

HRID 873950 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)C(=O)CC(C)=O
HCID69208

Ethyl 2,4-dioxovalerate

C7H10O4

结构：O=Cc1cccc(OC(F)(F)F)c1
HCID605139

3-(Trifluoromethoxy)benzaldehyde

C8H5F3O2

结构：Cc1cc(N)cn(C)c1=O
HCID67456616

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)C1C(=O)C(=O)N(c2cc(C)c(=O)n(C)c2)C1c1cccc(OC(F)(F)F)c1
HCID117702800

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 57.1 using 5-amino-1,3-dimethylpyridin-2(1H)-one (Step 20.2), 3-trifluoromethoxy-benzaldehyde and ethyl acetopyruvate at 110° C. for 4 hr. tR: 0.79 min (LC-MS 2); ESI-MS: 423 [M+H]+ (LC-MS 2); ESI-MS: 421 [M−H]− (LC-MS 2).