HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)benzaldehyde → HCID 117702571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)benzaldehyde | HCID 67990 | — |
| Reactant | Ethyl 2,4-dioxovalerate | HCID 69208 | — |
| Reactant | 5-Amino-1,3-dimethyl-1,2-dihydropyridin-2-one | HCID 67456616 | — |
| Product | HCID 117702571 | HCID 117702571 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 57.1 using 5-amino-1,3-dimethylpyridin-2(1H)-one (Step 20.2), 3-trifluormethylbenzaldehyde and ethyl acetopyruvate. tR: 0.76 min (LC-MS 2); ESI-MS: 407 [M+H]+ (LC-MS 2); ESI-MS: 405 [M−H]− (LC-MS 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975417B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-5a71ffd31a754e6080bfa69f2dad8617 |
| Source note | uspto-grants-2015_03 |