HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 67071573, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 67071421 | HCID 67071421 | — |
| Product | HCID 67071573 | HCID 67071573 | — |
Reaction Steps
(−)-(E)-3-[4-Oxo-spiro(chromane-2,3′-pyrrolidine)-6-yl]-acrylic acid methyl ester (110 mg, 0.38 mmol) was treated with benzaldehyde and NaBH(OAc)3 according to the procedure used for Example 2, Step A to give (+)-(E)-3-[1′benzyl-4-oxo-spiro(chromane-2,3′-pyrrolidine)-6-yl]-acrylic acid methyl ester (45 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08980877B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-4263e9362adf49f79cf0caaad4b37986 |
| Source note | uspto-grants-2015_03 |