Hydrochloric Acid → HCID 90387564, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of Example 82a (0.1163 g, 0.31 mmol) in methanol (3.1 mL) was treated with hydrogen chloride solution (4 M in 1,4-dioxane) (1.55 mL, 6.2 mmol) and heated at 75° C. overnight and then for another 10 hours at 67° C. The reaction mixture was concentrated to give 0.151 g (>100%) of the title compound as the HCl salt

Provenance & Evidence