Myristyl bromide → HCID 12361490, compound

Participants

Reaction Steps

The product was generated using general protocol D using dimethyl-5-hydroxyisophthalate (1.037 g, 4.93 mmol), 1-bromotetradecane (1.34 mL, 4.48 mmol), K2CO3 (2.48 g, XXmol), CH3CN (50 mL) yielded 1.21 g (60.2%) of a white solid. 1H NMR (CDCl3, 400 MHz) δ: 8.2607 (s, 1H, Ar—H), 7.7396 (s, 2H, Ar—H), 4.0315 (t, 2H, O—CH2, 3J=6.62 Hz), 3.9374 (s, 6H, COOCH3), 1.8046 (p, 2H, O—CH2—CH23J=6.82 Hz), 1.4660 (p, 2H, O—CH2—CH2—CH2, 3J=6.86 Hz), 1.2582 (m, 22H), 0.8809 (t, 3H, CH2—CH3, 3J=6.69 Hz

Provenance & Evidence