HCID 12361490, compound → HCID 67507886, compound

Participants

Reaction Steps

The product was generated using general protocol E using dimethyl-5-tetradecyloxyisophthalate (D9, 1.171 g, 2.88 mmol), lithium aluminum hydride (0.253 g, 6.34 mmol), Et2O (40 mL) yielded 0.538 g (53.3%) of a white solid. 1H NMR (CDCl3, 300 MHz) δ: 6.9336 (s, 1H, Ar—H), 6.8501 (s, 2H, Ar—H), 4.6821 (s, 4H, Ar—CH2), 3.9708 (t, 2H, O—CH2, 3J=6.58 Hz), 1.7784 (p, 2H, O—CH2—CH2, 3J=7.16 Hz), 1.6328 (t, 2H, O—H), 1.4483 (p, 2H, O—CH2—CH2—CH2, 3J=7.58 Hz), 1.2625 (m, 20H), 0.8810 (t, 3H, CH2—CH3, 3J=6.83 Hz).

Provenance & Evidence