HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-methoxyphenyl)piperazine → HCID 53327887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-methoxyphenyl)piperazine | HCID 81430 | — |
| Reactant | 3-(5-(Trifluoromethyl)-1,2,4-oxadiazol-3-yl)benzoic acid | HCID 25180854 | — |
| Product | HCID 53327887 | HCID 53327887 | 49% |
Reaction Steps
This compound was synthesized from 1-(3-methoxyphenyl)piperazine and 3-(5-(trifluoromethyl)-1,2,4-oxadiazol-3-yl)benzoic acid as described for example 37 step 3 (110 mg, yield 49%). 1H NMR (400 MHz, CDCl3) δ 8.22-8.20 (m, 2H), 7.67-7.60 (m, 2H), 7.23-7.19 (m, 1H), 6.57-6.54 (m, 1H), 6.49-6.48 (m, 2H), 3.98 (m, 2H), 3.80 (s, 3H), 3.61 (m, 2H), 3.30-3.16 (m, 4H). MS (ESI) m/z: Calculated for C21H18F3N4O3: 432.14. found: 433.2 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08981084B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-2493e63bb04d43bcb1ca00119c585413 |
| Source note | uspto-grants-2015_03 |