Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetonitrile → 3-(3-(3-Benzyloxy-propoxy)-phenyl)-3-hydroxy-propionitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetonitrile | HCID 6342 | — |
| 반응물 | 3-(3-(Benzyloxy)propoxy)benzaldehyde | HCID 86637622 | — |
| 생성물 | 3-(3-(3-Benzyloxy-propoxy)-phenyl)-3-hydroxy-propionitrile | HCID 67316970 | — |
반응 단계
Addition of acetonitrile to 3-(3-benzyloxy-propoxy)-benzaldehyde gave 3-(3-(3-benzyloxy-propoxy)-phenyl)-3-hydroxy-propionitrile as yellow oil. Yield (0.94 g, 54%): 1H NMR (400 MHz, CDCl3) δ 7.23-7.38 (m, 6H), 6.90-6.96 (m, 2H), 6.81-6.86 (m, 1H), 5.00 (m, 1H), 4.53 (s, 2H), 4.10 (t, J=6.2 Hz, 2H), 3.67 (t, J=6.0, 2H), 2.75 (t, J=6.4, 2H), 2.04-2.13 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08981153B2 |
| 출처 데이터셋 | uspto-grants-2015_03 |
| ORD ID | ord-6f6850593a464a3499a02639ce6b0669 |
| 출처 메모 | uspto-grants-2015_03 |