Ethanolamine → HCID 53259297, compound

Participants

Reaction Steps

53 mg of 2-fluoro-N-(4-phenoxyphenyl)pyridin-4-amine in 80.6 mg of ethanolamine were heated in a screw cap vial under argon at 150° C. for 3 days. The mixture obtained was cooled to r.t. and 5 mL of 2N NaOH were added. The mixture obtained was extracted with 15 mL of EtOAc for three times. From the mixture obtained organic solvent was evaporated off. 2-(4-(4-Phenoxyphenylamino)pyridin-2-ylamino)ethan-1-ol was obtained.

Provenance & Evidence