1-(5-Propyl-1,3-benzodioxol-2-yl)ethanone → HCID 67111420, compound

HRID 876198Notes

Reaction equation

HRID 876198 reaction equation
[CH2:1]([C:4]1[CH:15]=[CH:14][C:7]2[O:8][CH:9]([C:11](=[O:13])[CH3:12])[O:10][C:6]=2[CH:5]=1)CC.[CH2:16]([Li])C>>[CH3:1][C:4]1[CH:15]=[CH:14][C:7]2[O:8][CH:9]([C:11](=[O:13])[CH2:12][CH3:16])[O:10][C:6]=2[CH:5]=1

Participants

3

Reactant 2

HCID 669810371-(5-Propyl-1,3-benzodioxol-2-yl)ethanoneHCID 178506846HCID 178506846, compound

Product 1

HCID 67111420HCID 67111420, compound

Procedure

Obtained in 30% (1st step) and 33% (2nd step) yields from 4-methylcatechol according to the typical procedure described for 1-(5-propyl-1,3-benzodioxol-2-yl)-1-ethanone, except the use of ethyl lithium instead of methyl lithium.

Sources & evidence

ORD record
ord-ea1c74c93fc848068e63b4825e03cc0f
Source dataset
uspto-grants-2015_03
Patent number
US08987188B2

Reaction notes

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