HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dibromo-2-methylpyridine → 3-Bromo-5-(4-ethylphenyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dibromo-2-methylpyridine | HCID 619705 | — |
| Reactant | Boronic acid, (4-ethylphenyl)- | HCID 2734352 | — |
| Product | 3-Bromo-5-(4-ethylphenyl)pyridine | HCID 66520574 | — |
Reaction Steps
23 g (97 mmol) of methyl 3,5-dibromopyridine and 18 g (117 mmol, 1.2 eq.) of 4-ethylphenylboronic acid were reacted according to General Method 1A. Yield: 17 g (66% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987248B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-c4e2854dadfe460b80c54b97842f284e |
| Source note | uspto-grants-2015_03 |