HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methyl-1-piperazinecarbonyl chloride → HCID 66701421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methyl-1-piperazinecarbonyl chloride | HCID 3016935 | — |
| Reactant | 5-(4-ethylphenyl)-N-phenylpiperidine-3-carboxamide | HCID 66701553 | — |
| Product | HCID 66701421 | HCID 66701421 | — |
Reaction Steps
250 mg (0.74 mmol) of 5-(4-ethylphenyl)-N-phenylpiperidine-3-carboxamide (Example 17A) and 156 mg (0.96 mmol, 1.3 eq.) of 4-methylpiperazine-1-carbonyl chloride were reacted according to General Method 3. Yield: 213 mg (66% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987248B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-ffb74b0bb8ee408b861d86955e71b537 |
| Source note | uspto-grants-2015_03 |