HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butylsulfinamide, (R)-(+)- → HCID 140636148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butylsulfinamide, (R)-(+)- | HCID 10964479 | — |
| Reactant | 2-Fluoro-1-(2-fluoro-phenyl)-ethanone | HCID 21964491 | — |
| Product | HCID 140636148 | HCID 140636148 | 62% |
Reaction Steps
In a manner analogous to that described for the preparation of sulfinyl imine E2.1 the reaction of 2-fluoro-1-(2-fluoro-phenyl)-ethanone with (R)-tert-butylsulfinamide yielded the (R)-2-methyl-propane-2-sulfinic acid [2-fluoro-1-(2-fluoro-phenyl)-eth-(E)-ylidene]-amide (62% yield) as an orange oil. MS (ISP): m/z=260.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987255B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-17811615fb5c4fbc90855a24aa3db7a7 |
| Source note | uspto-grants-2015_03 |