1,4-Dioxane hydrochloride → HCID 58181607, compound

Participants

Reaction Steps

To round bottom flask charged with the compound 71-2 (50 mg) at rt was added 4 N HCl/dioxane (3 mL). The resulting solution was stirred for 3 h, concentrated under reduced pressure, and placed under high vacuum. The crude product was dissolved in MeOH and Et2O and the resultant solid was collected and dried to afford EXAMPLE 71 (36 mg) as an off-white solid. LC-MS: M+H=425 (free base).

Provenance & Evidence