反应详情

温度

90 °C

45.0 g (302.1 mmol) 4,6-dichloropyrimidine are initially introduced into 450 ml water. 26.3 g (302.1 mmol) morpholine are added and the mixture is stirred at 90° C. for 16 h. Thereafter, it is cooled to 0° C. and the precipitate formed is filtered off. The precipitate is washed once with 50 ml water and dried in air.

1. temperatureThereafter, it is cooled to 0° C.
2. customthe precipitate formed
3. filtrationis filtered off
4. washThe precipitate is washed once with 50 ml water
5. customdried in air