HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → HCID 136080218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 67446824 | HCID 67446824 | — |
| Product | HCID 136080218 | HCID 136080218 | — |
Reaction Steps
Reaction of 5-benzyloxy-6-[5-(4-fluoro-benzyl)-[1,3,4]oxadiazol-2-yl]-3-methyl-3H-pyrimidin-4-one and a 1:1 mixture of TFA/CH2Cl2 gave the debenzylated product in reasonable yield. Results are summarized below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987272B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-f1ff02f22305415d8936ec4cce9193ff |
| Source note | uspto-grants-2015_03 |