HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 876813Generated: October 28, 2026
O-(2,4-dinitrophenyl)hydroxylamine → HCID 86671435, compound
https://huagongshe.com/reaction/876813
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | O-(2,4-dinitrophenyl)hydroxylamine | HCID 87140 | — |
| Reactant | 4-(Tert-butyldimethylsilyloxymethyl)pyridine | HCID 10987880 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86671435 | HCID 86671435 | 203.9% |
Reaction Steps
A mixture of 4-((tert-butyldimethylsilyloxy)methyl)pyridine (8.9 g, 39.7 mmol) and O-(2,4-dinitrophenyl)hydroxylamine Y-3 (7.9 g, 39.7 mmol) in MeCN (27 ml) was stirred at 40° C. for 24 h, then concentrated to afford the title compound (17.1 g), used in next step without further purification. MS (m/z): 239(M−183)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08987269B2 |
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| Source dataset | uspto-grants-2015_03 |
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| ORD ID | ord-0508233c344e463d83bd9bec355dd36c |
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| Source note | uspto-grants-2015_03 |
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