HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-(Azidomethyl)[1,2,4]triazolo[1,5-a]pyridine → HCID 68288052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-(Azidomethyl)[1,2,4]triazolo[1,5-a]pyridine | HCID 86671437 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68288052 | HCID 68288052 | 106.6% |
Reaction Steps
To a solution of 7-(azidomethyl)-[1,2,4]triazolo[1,5-a]pyridine (4-4) (340 mg, 1.9 mmol) in methanol (20 mL) was added Pd/C (30 mg). The reaction mixture was stirred at room temperature under H2 (1 atm) for 2 h. The mixture was filtered to remove Pd/C. The filtrate was concentrated to afford the title compound (300 mg) MS (m/z): 149 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987269B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-2b7a75afe6bc43f9becd18c07d819f59 |
| Source note | uspto-grants-2015_03 |