HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 88922490, compound → HCID 68285281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 88922490 | HCID 88922490 | — |
| Solvent | Hydrochloride methanol | HCID 21893726 | — |
| Product | HCID 68285281 | HCID 68285281 | — |
Reaction Steps
A solution of compound 330-a (300 mg) in 10 mL of HCl/CH3OH was stirred overnight, then concentrated and basified with Na2CO3 solution. The resulting mixture was purified by chromatography to afford the title compound as a solid, 155 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987269B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-8baf321d60db4cf89d298519b2cc3da1 |
| Source note | uspto-grants-2015_03 |