HCID 58136345, compound → HCID 58136315, compound

Participants

Reaction Steps

765 mg (2.63 mmol) of tert-butyl 1-(2-methyl-3-nitrobenzyl)cyclopropanecarboxylate were dissolved in 5 ml of ethanol, and 139.7 mg (0.13 mmol) of palladium (10% on carbon) were added. At RT, the mixture was hydrogenated at atmospheric pressure for 2 h. The reaction mixture was filtered off with suction through kieselguhr, the residue was washed with THF and the filtrate was concentrated. This gave 680 mg (99.1% of theory) of the title compound.

Provenance & Evidence