HCID 24950528, compound → HCID 24948911, compound

Participants

Reaction Steps

The title compound was prepared from 13f (1.9 mg, 0.0047 mmol) following general procedure A. Tritration with Et2O afforded the title compound (1.3 mg, 71%) as a white solid: 1H NMR (CDCl3, 600 MHz) δ 9.06 (d, 1H, J=7.8 Hz), 8.65 (d, 1H, J=8.7 Hz), 8.42 (d, 1H, J=7.5 Hz), 8.32 (d, 1H, J=8.7 Hz), 8.23 (t, 1H, J=7.8 Hz), 7.27 (m, 2H), 7.17 (m, 3H), 3.45 (t, 2H, J=7.4 Hz), 2.62 (t, 2H, J=7.8 Hz), 1.83 (m, 2H), 1.66 (m, 2H), 1.46 (m, 4H); 13C NMR (CDCl3, 150 MHz) δ 200.2, 163.5, 158.2, 155.7, 152.2, 146.4, 142.9, 140.2, 128.5, 128.4, 126.7, 126.0, 125.8, 125.7, 125.2, 38.5, 36.1, 31.5, 29.3, 29.2, 24.0; HRMS-ESI-TOF m/z 390.1811 ([M+H]+, C23H23N3O3 requires 390.1812).

Provenance & Evidence