HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(4-Methoxy-2-methylphenyl)boronic acid → N-[4-(4-Methoxy-2-methyl-phenyl)-pyridin-3-yl]-N-methyl-3,5-bis-trifluoromethyl-benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (4-Methoxy-2-methylphenyl)boronic acid | HCID 2773486 | — |
| Edukt | N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide | HCID 86670692 | — |
| Produkt | N-[4-(4-Methoxy-2-methyl-phenyl)-pyridin-3-yl]-N-methyl-3,5-bis-trifluoromethyl-benzamide | HCID 60197296 | — |
Reaktionsschritte
The title compound was prepared in analogy to example 25, from N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide (example 25, intermediate a) and 4-methoxy-2-methylphenylboronic acid (CAS RN 208399-66-0). Pale yellow sticky solid (67%). MS (ESI): m/z=469.2 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08987307B2 |
| Quelldatensatz | uspto-grants-2015_03 |
| ORD ID | ord-cec6c808e59b458ead2134d45ebb628f |
| Quellennotiz | uspto-grants-2015_03 |