HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluorophenylboronic acid → HCID 60196807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluorophenylboronic acid | HCID 2734334 | — |
| Reactant | N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide | HCID 86670692 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 60196807 | HCID 60196807 | — |
Reaction Steps
The title compound was prepared in analogy to example 25, from N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide (example 25, intermediate a) and 2,4-difluorophenylboronic acid (CAS RN 144025-03-6) and using DMF as reaction solvent. Off-white solid (60%). MS (ESI): m/z=461.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987307B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-19a583a5f4f441e28f5b00dce42a4e8e |
| Source note | uspto-grants-2015_03 |