HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Fluoro-6-methoxyphenyl)boronic acid → HCID 60196701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Fluoro-6-methoxyphenyl)boronic acid | HCID 3294524 | — |
| Reactant | N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide | HCID 86670692 | — |
| Product | HCID 60196701 | HCID 60196701 | — |
Reaction Steps
The title compound was prepared in analogy to example 58, from N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide (example 25, intermediate a) and 2-fluoro-6-methoxy-phenylboronic acid (CAS RN 78495-63-3) and using preparative HPLC for the chromatographic purification. Off-white solid (36%). MS (ESI): m/z=473.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987307B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-514175220d9b49cfa9a6912b9f58d810 |
| Source note | uspto-grants-2015_03 |