3,5-Bis(trifluoromethyl)benzoyl chloride → HCID 86670747, compound

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Reaction Steps

The title compound was prepared in analogy to example 72, intermediate, from {2-[4-(2-chloro-phenyl)-pyridin-3-ylamino]ethyl}-carbamic acid benzyl ester and 3,5-bis(trifluoromethyl)benzoyl chloride (CAS RN 1271-19-8) and using a gradient of n-heptane:EtOAc (100:0 to 0:100) for the chromatographic purification. Light brown solid (36%). MS (ESI): m/z=622.13 [M+H]+.

Provenance & Evidence