HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorophenylboronic acid → HCID 86670767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorophenylboronic acid | HCID 2734354 | — |
| Reactant | HCID 60198028 | HCID 60198028 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 86670767 | HCID 86670767 | — |
Reaction Steps
The title compound was prepared in analogy to example 72, from (2,2-difluoro-ethyl)-(4-iodo-pyridin-3-yl)-amine (example 153, intermediate b) and 2-fluorophenylboronic acid (CAS RN 1193-03-9) and using a gradient of n-heptane:EtOAc (100:0 to 50:50) for the chromatographic purification. Colorless solid (87%). MS (ESI): m/z=252.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987307B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-6c5300a2bc18480081c6d709946cfb22 |
| Source note | uspto-grants-2015_03 |