HRID878256

反应详情

EQUATION

反应方程式

HRID 878256 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in analogy to example 72, intermediate, from [4-(2-fluoro-6-methoxy-phenyl)-pyridin-3-yl]-(2,2,2-trifluoro-ethyl)-amine and 3-methanesulfonyl-5-trifluoromethyl-benzoyl chloride after a reaction time of 12 hours. The compound was purified by preparative HPLC (ammonium acetate/acetonitril e). Off-white solid (27%). MS (ESI): m/z=551.1 [M+H]+.

WORKUP

后处理

  1. customThe compound was purified by preparative HPLC (ammonium acetate/acetonitril e)