HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-cyclopropyl-3-oxopropanoate → HCID 178524558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-cyclopropyl-3-oxopropanoate | HCID 262979 | — |
| Reactant | 2-Hydrazinylpyridine-4-carboxylic acid | HCID 26967246 | — |
| Product | HCID 178524558 | HCID 178524558 | 24% |
Reaction Steps
The title compound was prepared in 24% yield from 2-hydrazinylpyridine-4-carboxylic acid and ethyl 3-cyclopropyl-3-oxopropanoate according to the procedure for the preparation of Example 1. 1H NMR (400 MHz, CD3OD): δ 0.83-0.88 (2H, m), 1.05-1.09 (2H, m), 1.88-1.91 (1H, m), 4.86 (1H, s), 7.70 (1H, dd, J=5.2, 1.2 Hz), 8.54 (1H, d, J=5.2 Hz), 8.75 (1H, s). [M+H] Calc'd for C12H11N3O3, 246; Found, 246.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987461B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-8a01e586607246349465f37eca2ae956 |
| Source note | uspto-grants-2015_03 |