3-Methoxybenzyl alcohol → HCID 86725514, compound

HRID 878542Notes

Reaction equation

HRID 878542 reaction equation
[OH:1][C:2]1[N:6]([C:7]2[CH:12]=[C:11]([C:13]#[N:14])[CH:10]=[CH:9][N:8]=2)[N:5]=[CH:4][CH:3]=1.[CH3:15][O:16][C:17]1[CH:18]=[C:19]([CH:22]=[CH:23][CH:24]=1)[CH2:20]O>>[CH3:15][O:16][C:17]1[CH:18]=[C:19]([CH:22]=[CH:23][CH:24]=1)[CH2:20][O:1][C:2]1[N:6]([C:7]2[CH:12]=[C:11]([C:13]#[N:14])[CH:10]=[CH:9][N:8]=2)[N:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 814373-Methoxybenzyl alcoholHCID 178510213HCID 178510213, compound

Product 1

HCID 86725514HCID 86725514, compoundYield 13%

Procedure

The title compound was prepared in 13% yield from 2-(5-hydroxy-1H-pyrazol-1-yl)pyridine-4-carbonitrile and 3-methoxybenzyl alcohol according to the procedure for the preparation of Example 39, part C. [M+H] Calc'd for C17H14N4O2, 307; Found, 307.

Sources & evidence

ORD record
ord-935a0a92c4854d9dad026eeba6727b07
Source dataset
uspto-grants-2015_03
Patent number
US08987461B2

Reaction notes

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