2-Hydrazinylpyridine-4-carbonitrile → HCID 86725548, compound

HRID 878581Notes

Reaction equation

HRID 878581 reaction equation
C[N:2](/[CH:4]=[C:5](\[CH2:11][CH3:12])/[C:6]([O:8][CH2:9][CH3:10])=[O:7])C.[NH:13]([C:15]1[CH:20]=[C:19]([C:21]#[N:22])[CH:18]=[CH:17][N:16]=1)N>>[C:21]([C:19]1[CH:18]=[CH:17][N:16]=[C:15]([NH:13][NH:2]/[CH:4]=[C:5](\[CH2:11][CH3:12])/[C:6]([O:8][CH2:9][CH3:10])=[O:7])[CH:20]=1)#[N:22]

Participants

3

Reactant 2

HCID 201187142-Hydrazinylpyridine-4-carbonitrileHCID 86725547HCID 86725547, compound

Product 1

HCID 86725548HCID 86725548, compound

Procedure

The title compound was prepared from ethyl (2E)-2-(dimethylaminomethylidene)butanoate and 2-hydrazinylpyridine-4-carbonitrile (PREPARATION 2) according to the procedure for the preparation of Example 84, part B. [M+H] Calc'd for C13H16N4O2, 261; Found, 261.

Workup

  1. customaccording to the procedure for the preparation of Example 84, part B

Sources & evidence

ORD record
ord-09f138d62574466f98b55a37eda2f88c
Source dataset
uspto-grants-2015_03
Patent number
US08987461B2

Reaction notes

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