HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorostyrene → [4-chloro-2-[(E)-2-(4-fluorophenyl)ethenyl]phenyl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorostyrene | HCID 67883 | — |
| Reactant | (2-Bromo-4-chlorophenyl)methanol | HCID 54049764 | — |
| Product | [4-chloro-2-[(E)-2-(4-fluorophenyl)ethenyl]phenyl]methanol | HCID 86725610 | — |
Reaction Steps
The title compound was prepared from (2-bromo-4-chlorophenyl)methanol and 4-fluoro-1-vinylbenzene according to the procedure for the preparation of Example 119, part B. 1H NMR (400 MHz, CDCl3): δ 1.72 (1H, t, J=5.6 Hz), 4.77 (2H, d, J=5.2 Hz), 6.98-7.08 (3H, m), 7.22-7.34 (3H, m), 7.47-7.50 (2H, m), 7.60 (1H, d, J=1.6 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987461B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-12be53f4989741eea0ed8e2e397d2429 |
| Source note | uspto-grants-2015_03 |