trans-2-Decenoic acid → HCID 86694799, compound

HRID 878874Notes

Reaction equation

HRID 878874 reaction equation
[C:1]([OH:12])(=[O:11])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH2:13]([N:15]([CH2:23][CH3:24])[CH2:16][CH2:17][O:18][CH2:19][CH2:20][CH2:21]O)[CH3:14]>>[C:1]([O:12][CH2:21][CH2:20][CH2:19][O:18][CH2:17][CH2:16][N:15]([CH2:23][CH3:24])[CH2:13][CH3:14])(=[O:11])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 5282724trans-2-Decenoic acidHCID 18935974HCID 18935974, compound

Product 1

HCID 86694799HCID 86694799, compound

Procedure

The same operation as in Example 1-1 or 1-2 was carried out using trans-2-decenoic acid and 3-(2-(diethylamino)ethoxy)propan-1-ol as starting materials to give the aimed compound. Compound 14 was obtained by the purification using silica gel column chromatography.

Sources & evidence

ORD record
ord-3d71f39cc100404bbe35c13f3e9f0bc9
Source dataset
uspto-grants-2015_03
Patent number
US08987486B2

Reaction notes

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