1-Heptanethiol → (E)-S-heptyl dec-2-enethioate

HRID 878909Notes

Reaction equation

[C:1]([OH:12])(=O)/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH2:13]([SH:20])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]>>[C:1](=[O:12])([S:20][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

Reactant 2

HCID 154221-Heptanethiol

HCID 5282724trans-2-Decenoic acid

Product 1

HCID 86694816(E)-S-heptyl dec-2-enethioate

Procedure

The same operation as in Example 1-1 or 1-2 was carried out using trans-2-decenoic acid and 1-heptanethiol as starting materials to give the aimed compound.

Sources & evidence

ORD record: ord-68ae046de3ae4353a02451a4f1b186e7
Source dataset: uspto-grants-2015_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08987486B2

Reaction notes

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