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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 879023Generated: October 25, 2026

Triethylamine → Benzyl 4-chlorobenzoyloxycarbamate

https://huagongshe.com/reaction/879023

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant4-Chlorobenzoyl chlorideHCID 8501—
ReactantBenzyl hydroxycarbamateHCID 18907—
SolventDiethyl EtherHCID 3283—
ProductBenzyl 4-chlorobenzoyloxycarbamateHCID 51033117—

Reaction Steps

4-Chlorobenzoyl chloride (13.1 mL, 102 mmol) is added slowly to a solution of benzyl hydroxycarbamate (19.0 g, 114 mmol) and triethylamine (14.4 mL, 104 mmol) in diethyl ether (500 mL) at 0° C. then stirred at room temperature for 1 h. The reaction is

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08987504B2
Source datasetuspto-grants-2015_03
ORD IDord-61ae2cfa3efb4b06b28f8c9207977e98
Source noteuspto-grants-2015_03