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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 879538Generated: October 30, 2026

HCID 86700358, compound → HCID 86700360, compound

https://huagongshe.com/reaction/879538

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86700358HCID 86700358—
SolventHydrochloric AcidHCID 313—
SolventIsopropanolHCID 3776—
ProductHCID 86700360HCID 86700360—

Reaction Steps

A solution of (R)-tert-butyl 3-(6-(6-((S)-1-tert-butoxy-2-ethoxy-2-oxoethyl)-7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-2-yl)-2-methyl-1H-benzo[d]imidazol-1-yl)pyrrolidine-1-carboxylate (77 mg, 0.11 mmol) in 1.25 M HCl in i-PrOH (12 mL) was stirred at room temperature for 16 hours. The solution was then concentrated in vacuo to provide the desired product. LCMS-ESI+: calc'd for C34H38ClN4O3S: 617.2 (M+H+); Found: 617.2 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08987250B2
Source datasetuspto-grants-2015_03
ORD IDord-2e6c938426304b14bb74f0cd3e807efe
Source noteuspto-grants-2015_03