HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzotriazole → HCID 86700391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzotriazole | HCID 71757472 | — |
| Reactant | HCID 86700215 | HCID 86700215 | — |
| Product | HCID 86700391 | HCID 86700391 | — |
Reaction Steps
Prepared in a manner similar to (S)-ethyl 2-tert-butoxy-2-(7-(4-chlorophenyl)-5-methyl-2-(1-methyl-1H-benzo[d][1,2,3]triazol-5-yl)benzo[d]thiazol-6-yl)acetate, but using 1-methyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzo[d][1,2,3]triazole instead of 1-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzo[d][1,2,3]triazole. 1H NMR (400 MHz, CDCl3) δ 8.46 (s, 1H), 8.11 (d, J=8.7 Hz, 1H), 7.96 (d, J=7.6 Hz, 2H), 7.60-7.45 (m, 4H), 5.18 (s, 1H), 4.39 (s, 3H), 4.28-4.17 (m, 2H), 2.63 (s, 3H), 1.26 (t, J=8 Hz, 3H), 0.99 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987250B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-edc307ed51a44181aaa4a6aa343a82dc |
| Source note | uspto-grants-2015_03 |