HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86700216, compound → HCID 86700403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86700216 | HCID 86700216 | — |
| Reactant | HCID 86700401 | HCID 86700401 | — |
| Product | HCID 86700403 | HCID 86700403 | — |
Reaction Steps
Prepared in a manner similar to (S)-2-tert-butoxy-2-(7-(4-chlorophenyl)-5-methyl-2-(1-methyl-1H-benzo[d][1,2,3]triazol-5-yl)benzo[d]thiazol-6-yl)acetic acid, but using (S)-ethyl 2-tert-butoxy-2-(7-(4-chlorophenyl)-2-(1,3-dimethylimidazo[1,5-a]pyridin-7-yl)-5-methylbenzo[d]thiazol-6-yl)acetate instead of (S)-ethyl 2-tert-butoxy-2-(7-(4-chlorophenyl)-5-methyl-2-(1-methyl-1H-benzo[d][1,2,3]triazol-5-yl)benzo[d]thiazol-6-yl)acetate. LCMS-ESI+: calc'd for C29H29ClN3O3S: 534.1 (M+H+); Found: 534.2 (M+H+). 1H NMR (400 MHz, CD3OD) δ 8.33 (s, 1H), 8.28 (d, J=7.7 Hz, 1H), 7.87 (s, 1H), 7.76-7.65 (m, 2H), 7.60 (d, J=6.4 Hz, 3H), 5.27 (s, 1H), 2.86 (s, 3H), 2.65 (s, 3H), 2.62 (s, 3H), 0.98 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987250B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-c63ba9a8d65f4d3bbbb92e35a306686f |
| Source note | uspto-grants-2015_03 |