HCID 63893933, compound → HCID 86700412, compound

Participants

Reaction Steps

(S)-2-tert-butoxy-2-(7-(4-chlorophenyl)-2-(3-isopropyl-1-methyl-1H-indazol-5-yl)-5-methylbenzo[d]thiazol-6-yl)acetic acid was prepared in a similar manner as (S)-2-tert-butoxy-2-(7-(4-chlorophenyl)-5-methyl-2-(1-methyl-3-(pyridin-3-yl)-1H-indazol-5-yl)benzo[d]thiazol-6-yl)acetic acid except 1-(5-bromo-2-fluorophenyl)-2-methylpropan-1-ol was used instead of (5-bromo-2-fluorophenyl)(pyridin-3-yl)methanol. LCMS-ESI+: calc'd for C31H33ClN3O3S: 562.2 (M+H+); Found 562.3 (M+H+). 1H NMR (400 MHz, CD3OD) δ 8.44 (s, 1H), 8.03 (dd, J=8.9, 1.6 Hz, 1H), 7.81 (s, 1H), 7.70 (d, J=8.3 Hz, 1H), 7.58 (dd, J=9.4, 6.9 Hz, 4H), 5.26 (s, 1H), 4.01 (s, 3H), 3.45 (hept, J=7.0 Hz, 1H), 2.61 (s, 3H), 1.46 (d, J=7.0 Hz, 6H), 0.98 (s, 9H).

Provenance & Evidence