Ethanol → HCID 5370806, compound

Participants

Reaction Conditions

Reaction Steps

64.7 g (0.43 mol) of 2-nitrobenzaldehyde and 105.7 g (0.43 mol) of 4-bromophenylacetic acid sodium salt are dissolved in 500 ml of acetic anhydride and stirred at 80° C. for 2 h. When the reaction is complete, the mixture is extended with 1000 ml of water and 750 ml of EtOH and heated to 110° C., and, after 20 min, the orange solid is filtered off with suction, washed with water and MeOH and dried, giving 107 g (71.8%) of a yellow powder.

Provenance & Evidence