HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodoaniline → HCID 136352200, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodoaniline | HCID 12271 | — |
| Reactant | Sodium (4-morpholin-4-yl-6-oxo-1,6-dihydropyrimidin-2-yl)acetate | HCID 136041844 | — |
| Product | HCID 136352200 | HCID 136352200 | 76.4% |
Reaction Steps
The product is prepared according to the procedure described in Example 5, using 268 mg of sodium [4-(morpholin-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl]acetate and 324 mg of 3-iodoaniline in place of the 2,4-difluoroaniline. 345 mg of N-(3-iodophenyl)-2-[4-(morpholin-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl]acetamide are obtained in the form of a white solid, the characteristics of which are the following:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993565B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-bd6991e9ef384e2891d195790d84ceb5 |
| Source note | uspto-grants-2015_03 |